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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2284298Generated: October 25, 2026

1-Methyl-1H-indole-5-carboxylic acid → N,N'-(Ethene-1,1-diylbis(4,1-phenylene))bis(1-methyl-1H-indole-5-carboxamide)

https://huagongshe.com/reaction/2284298

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Methyl-1H-indole-5-carboxylic acidHCID 7015601—
Reactant4,4'-(Ethene-1,1-diyl)dianilineHCID 15471336—
ProductN,N'-(Ethene-1,1-diylbis(4,1-phenylene))bis(1-methyl-1H-indole-5-carboxamide)HCID 67688251—

Reaction Steps

Compound 702 was prepared according to the procedure described in Scheme IV from 4,4′-(ethene-1,1-diyl)dianiline and 1-methylindole-5-carboxylic acid. 1H NMR (500 MHz, CDCl3) δ 8.20 (s, 2H), 7.93 (s, 2H), 7.79 (dd, J=1.7, 8.5 Hz, 2H), 7.66 (dd, J=1.7, 6.8 Hz, 4H), 7.42 (d, J=2.3 Hz, 2H), 7.39 (d, J=8.5 Hz, 4H), 7.15 (d, J=2.3 Hz, 2H), 6.61 (d, J=2.9 Hz, 2H), 5.44 (s, 2H), 3.86 (s, 6H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09144557B2
Source datasetuspto-grants-2015_09
ORD IDord-1e571aa3798947cda293a6bbaabc495a
Source noteuspto-grants-2015_09