4,4'-Diaminodiphenylamine → N,N'-(Azanediylbis(4,1-phenylene))bis(4-(4H-1,2,4-triazol-4-yl)benzamide)

HRID 2284299Notes

Reaction equation

HRID 2284299 reaction equation
[CH:1]1[C:6]([NH2:7])=[CH:5][CH:4]=[C:3]([NH:8][C:9]2[CH:14]=[CH:13][C:12]([NH2:15])=[CH:11][CH:10]=2)[CH:2]=1.[N:16]1[N:17]=[CH:18][N:19]([C:21]2[CH:29]=[CH:28][C:24]([C:25](O)=[O:26])=[CH:23][CH:22]=2)[CH:20]=1>>[NH:8]([C:3]1[CH:2]=[CH:1][C:6]([NH:7][C:25](=[O:26])[C:24]2[CH:28]=[CH:29][C:21]([N:19]3[CH:18]=[N:17][N:16]=[CH:20]3)=[CH:22][CH:23]=2)=[CH:5][CH:4]=1)[C:9]1[CH:14]=[CH:13][C:12]([NH:15][C:25](=[O:26])[C:24]2[CH:23]=[CH:22][C:21]([N:19]3[CH:20]=[N:16][N:17]=[CH:18]3)=[CH:29][CH:28]=2)=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 108414,4'-DiaminodiphenylamineHCID 31635814-(4H-1,2,4-triazol-4-yl)benzoic acid

Product 1

HCID 67113044N,N'-(Azanediylbis(4,1-phenylene))bis(4-(4H-1,2,4-triazol-4-yl)benzamide)

Procedure

Compound 747 was prepared according to the procedure described in Scheme IV from 4,4′-diaminodiphenylamine and 4-(4H-1,2,4-triazol-4-yl)benzoic acid. [M+H]+ calcd for C30H23N9O2: 542.20; found 541.99.

Sources & evidence

ORD record
ord-c9aae85dab434e3d8d4a21e7bf62bc89
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

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