4,4'-Diaminodiphenylamine → N,N'-(Azanediylbis(4,1-phenylene))bis(4-acetylbenzamide)

HRID 2284300Notes

Reaction equation

HRID 2284300 reaction equation
[CH:1]1[C:6]([NH2:7])=[CH:5][CH:4]=[C:3]([NH:8][C:9]2[CH:14]=[CH:13][C:12]([NH2:15])=[CH:11][CH:10]=2)[CH:2]=1.[C:16]([C:19]1[CH:27]=[CH:26][C:22]([C:23](O)=[O:24])=[CH:21][CH:20]=1)(=[O:18])[CH3:17]>>[NH:8]([C:3]1[CH:2]=[CH:1][C:6]([NH:7][C:23](=[O:24])[C:22]2[CH:26]=[CH:27][C:19]([C:16](=[O:18])[CH3:17])=[CH:20][CH:21]=2)=[CH:5][CH:4]=1)[C:9]1[CH:14]=[CH:13][C:12]([NH:15][C:23](=[O:24])[C:22]2[CH:21]=[CH:20][C:19]([C:16](=[O:18])[CH3:17])=[CH:27][CH:26]=2)=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 108414,4'-DiaminodiphenylamineHCID 114704-Acetylbenzoic Acid

Product 1

HCID 67687440N,N'-(Azanediylbis(4,1-phenylene))bis(4-acetylbenzamide)

Procedure

Compound 748 was prepared according to the procedure described in Scheme IV from 4,4′-diaminodiphenylamine and 4-acetylbenzoic acid. [M+H]+ calcd for C30H25N3O4: 492.18; found 492.00.

Sources & evidence

ORD record
ord-cc78a0577b244964b2666937a5cf4506
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

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