4,4'-Diaminodiphenylamine → N1,N1'-(Azanediylbis(4,1-phenylene))diterephthalamide

HRID 2284302Notes

Reaction equation

HRID 2284302 reaction equation
[CH:1]1[C:6]([NH2:7])=[CH:5][CH:4]=[C:3]([NH:8][C:9]2[CH:14]=[CH:13][C:12]([NH2:15])=[CH:11][CH:10]=2)[CH:2]=1.[C:16]([C:19]1[CH:27]=[CH:26][C:22]([C:23](O)=[O:24])=[CH:21][CH:20]=1)(=[O:18])[NH2:17]>>[NH:8]([C:3]1[CH:2]=[CH:1][C:6]([NH:7][C:23](=[O:24])[C:22]2[CH:26]=[CH:27][C:19]([C:16]([NH2:17])=[O:18])=[CH:20][CH:21]=2)=[CH:5][CH:4]=1)[C:9]1[CH:14]=[CH:13][C:12]([NH:15][C:23](=[O:24])[C:22]2[CH:26]=[CH:27][C:19]([C:16]([NH2:17])=[O:18])=[CH:20][CH:21]=2)=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 108414,4'-DiaminodiphenylamineHCID 5060574-Carbamoylbenzoic acid

Product 1

HCID 69674876N1,N1'-(Azanediylbis(4,1-phenylene))diterephthalamide

Procedure

Compound 754 was prepared according to the procedure described in Scheme IV from 4,4′-diaminodiphenylamine and 4-carbamoylbenzoic acid. [M+H]+ calcd for C28H23N5O4: 494.18; found 494.00.

Sources & evidence

ORD record
ord-877a6254c83e470a968c1778ff0d9c84
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

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