HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylethanediol → HCID 66726512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylethanediol | HCID 7996 | — |
| Reactant | 2,6-dichloropyridine-3,5-dicarbonitrile | HCID 850221 | — |
| Reactant | 1,3-Dihydro-1-hydroxy-2,1-benzoxaborol-5-ol | HCID 57968699 | — |
| Product | HCID 66726512 | HCID 66726512 | — |
Reaction Steps
This compound was prepared from 2,6-dichloropyridine-3,5-dicarbonitrile (obtained from Aces Pharma), 2-isopropoxyethanol, and benzo[c][1,2]oxaborole-1,5(3H)-diol in a similar manner to that of D230. 1H-NMR (400 MHz, DMSO-d6) δ (ppm) 1.0 (d, J=4.5 Hz, 6H), 3.42-3.45 (m, 1H), 3.49-3.51 (m, 2H), 4.14-4.16 (m, 2H), 5.01 (s, 2H), 7.3 (d, J=6.3 Hz, 1H), 7.39 (s, 1H), 7.81 (d, J=6.6 Hz, 1H), 8.94 (s, 1H), 9.28 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145429B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-d00bb7681f804c89ac763b7ceb6da97b |
| Source note | uspto-grants-2015_09 |