HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hydroxy-2-pentanone → HCID 66726518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hydroxy-2-pentanone | HCID 14066 | — |
| Reactant | 2,6-dichloropyridine-3,5-dicarbonitrile | HCID 850221 | — |
| Reactant | 1,3-Dihydro-1-hydroxy-2,1-benzoxaborol-5-ol | HCID 57968699 | — |
| Product | HCID 66726518 | HCID 66726518 | — |
Reaction Steps
This compound was prepared from 2,6-dichloropyridine-3,5-dicarbonitrile, 5-hydroxypentan-2-one, and benzo[c][1,2]oxaborole-1,5(3H)-diol in a similar manner to that of D230. 1H-NMR (400 MHz, DMSO-d6) δ (ppm) 1.7-1.73 (m, 2H), 2.04 (s, 3H), 2.35 (t, J=5.4 Hz, 2H), 4.06 (t, J=5.1 Hz, 2H), 5.02 (s, 2H), 7.29 (dd, J=6.3, 1.5 Hz, 1H), 7.39 (d, J=1.2 Hz, 1H), 7.81 (d, J=6.0 Hz, 1H), 8.94 (s, 1H), 9.3 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145429B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-20c7f31c1f0449e7965895fdf29dbe27 |
| Source note | uspto-grants-2015_09 |