HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylene Carbonate → 3,4-Ethylenedioxythiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylene Carbonate | HCID 7924 | — |
| Reactant | 2,2-Dimethoxy-2-phenylacetophenone | HCID 90571 | — |
| Reactant | Trifluoromethanesulfonic acid, lithium salt | HCID 3664839 | — |
| Product | 3,4-Ethylenedioxythiophene | HCID 4421864 | — |
Reaction Steps
Polymer Electrolyte: Five grams (g) of propylene carbonate, 5 g of poly(ethylene glycol)diacrylate (Mn=700), 1 g of lithium trifluoromethanesulfonate (“Litrif”), and 17.5 milligrams (mg) of dimethoxyphenylacetophenone (“DMPAP”) were added together and sonicated for 15 minutes until dissolved. The electrolyte is a colorless to light yellow liquid before UV exposure and a transparent gel afterwards. All chemicals were purchased from Sigma-Aldrich and used as received.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145515B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-4eb4f6109b414f2c93a280f8fcf1e5e4 |
| Source note | uspto-grants-2015_09 |