2-Methoxybenzoyl chloride → 4-(2-Hydroxybenzoyl)-2,3-dichlorophenetole

HRID 2285614Notes

Reaction equation

HRID 2285614 reaction equation
C[O:2][C:3]1[CH:11]=[CH:10][CH:9]=[CH:8][C:4]=1[C:5](Cl)=[O:6].[Cl:12][C:13]1[C:18]([Cl:19])=[CH:17][CH:16]=[CH:15][C:14]=1[O:20][CH2:21][CH3:22]>>[OH:2][C:3]1[CH:11]=[CH:10][CH:9]=[CH:8][C:4]=1[C:5]([C:17]1[CH:16]=[CH:15][C:14]([O:20][CH2:21][CH3:22])=[C:13]([Cl:12])[C:18]=1[Cl:19])=[O:6]

Participants

3

Reactant 2

HCID 889692-Methoxybenzoyl chlorideHCID 104200611,2-Dichloro-3-ethoxybenzene

Product 1

HCID 128540624-(2-Hydroxybenzoyl)-2,3-dichlorophenetole

Procedure

4-(2-Hydroxybenzoyl)-2,3-dichlorophenetole was prepared by reaction of 2-methoxybenzoyl chloride and 2,3-dichlorophenetole; m.p. of crude product 112°-120° C.

Workup

  1. customm.p. of crude product 112°-120° C.

Sources & evidence

ORD record
ord-d2dff68fd4aa4dfb9488e8dadaefa3f1
Source dataset
uspto-grants-1982_04
Patent number
US04323691

Reaction notes

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