HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → 5-Methyl-5-propyloxolan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | HCID 20543976 | HCID 20543976 | — |
| Product | 5-Methyl-5-propyloxolan-2-one | HCID 12322358 | 61% |
Reaction Steps
Using a method similar to Example 1, 186 parts of methyl 4-formyl-4-methyl-heptanoate are reacted with 80 parts of oxygen in the course of 5 hours. 86 parts (61% of theory) of γ-methyl-γ-propyl-γ-butyrolactone (boiling point 117°-119° C./20 mbar) are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04324727 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-74ae5217abac4d4da8efe56410f51ff2 |
| Source note | uspto-grants-1982_04 |