Acetic Anhydride → HCID 22623622, compound

HRID 2285675Notes

Reaction equation

HRID 2285675 reaction equation
[CH3:1][N:2]([CH3:7])[CH2:3][CH2:4]CO.[C:8]([O:11][C:12](=O)C)(=[O:10])[CH3:9]>>[C:8]([O:11][CH2:12][CH:3]([N:2]([CH3:1])[CH3:7])[CH3:4])(=[O:10])[CH3:9]

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 766463-(Dimethylamino)-1-propanol

Product 1

HCID 22623622HCID 22623622, compound

Procedure

14.4 g of 3-dimethylamino-1-propanol and 14.3 g of acetic anhydride are reacted and worked up as described in Example 7. Yield: 14.9 g (73.1%) of analytically pure product (analysis by gas chromatography) with a boiling point of 53° C./12 torr.

Sources & evidence

ORD record
ord-0eb6cb9ef94c47d89f627d200f448140
Source dataset
uspto-grants-1982_04
Patent number
US04324739

Reaction notes

Loading…