2-Methylbenzoyl chloride → HCID 21464720, compound

HRID 2285682Notes

Reaction equation

HRID 2285682 reaction equation
[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4](Cl)=[O:5].C[O:12][P:13]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([P:13](=[O:12])([C:20]1[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[O:5]

Participants

3

Reactant 2

HCID 702762-Methylbenzoyl chlorideHCID 77636Methoxydiphenylphosphine

Product 1

HCID 21464720HCID 21464720, compoundYield 84%

Procedure

Using a method similar to that of Example 2, 77 parts of 2-methyl-benzoic acid chloride and 108 parts of methoxydiphenylphosphine give 134 parts of 2-methylbenzoyldiphenylphosphine oxide. Yield 84% of theory, melting point 107° C.

Sources & evidence

ORD record
ord-0d267edecb194741b785ef36f3a3ff21
Source dataset
uspto-grants-1982_04
Patent number
US04324744

Reaction notes

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