Methoxydiphenylphosphine → HCID 21464710, compound

Participants

Reaction Steps

Using a method similar to that of Example 2, 80 parts of 1-methyl-1-cyclohexanecarboxylic acid chloride and 108 parts of methoxydiphenylphosphine, in the absence of a solvent, give 100 parts of 1-methyl-cyclohexylcarbonyl-diphenylphosphine oxide as an oily crude product, which is purified by chromatography over silica gel (using toluene as the eluant).

Provenance & Evidence