HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-enoyl chloride → HCID 178520429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
| Reactant | HCID 178517375 | HCID 178517375 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178520429 | HCID 178520429 | 65% |
Reaction Steps
7.5 g (0.05 moles) of 3-hydroxy-1,2-dihydro-pyrido[2,3-e]-as-triazine are reacted with 17 g (0.102 moles) of cinnamoyl chloride in 150 ml of acetonitrile as described in Example 6. 9.0 g (65%) of the title compound are obtained; m.p.: 221°-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04324786 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-eaf10b75564c481a9b0b02f10e8a1fc6 |
| Source note | uspto-grants-1982_04 |