2-Propanethiol → HCID 20544191, compound

HRID 2285714Notes

Reaction equation

HRID 2285714 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10]Cl)=[C:6]([C:12]([Cl:15])([Cl:14])[Cl:13])[CH:5]=1)([O-:3])=[O:2].[CH3:16][CH:17]([SH:19])[CH3:18]>>[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][S:19][CH:17]([CH3:18])[CH3:16])=[C:6]([C:12]([Cl:15])([Cl:14])[Cl:13])[CH:5]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 63642-PropanethiolHCID 127635554-Nitro-2-trichloromethylbenzenesulfenyl chloride

Product 1

HCID 20544191HCID 20544191, compoundYield 92.3%

Procedure

As in Example 1, 61 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride is reacted with 15 g of 2 -propylmercaptan. There is obtained 63 g (91% of theory) of (4-nitro-2-trichloromethylphenyl)-isopropyl disulfide.

Sources & evidence

ORD record
ord-288433cb31744b05ad5944aea33646cf
Source dataset
uspto-grants-1982_04
Patent number
US04324793

Reaction notes

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