Propyl mercaptan → HCID 20544193, compound

HRID 2285715Notes

Reaction equation

HRID 2285715 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10]Cl)=[C:6]([C:12]([Cl:15])([Cl:14])[Cl:13])[CH:5]=1)([O-:3])=[O:2].[CH2:16]([SH:19])[CH2:17][CH3:18]>>[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][S:19][CH2:16][CH2:17][CH3:18])=[C:6]([C:12]([Cl:15])([Cl:14])[Cl:13])[CH:5]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 7848Propyl mercaptanHCID 127635554-Nitro-2-trichloromethylbenzenesulfenyl chloride

Product 1

HCID 20544193HCID 20544193, compoundYield 90.8%

Procedure

Similarly, 61 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride is reacted with 15 g of 1-propylmercaptan. There is obtained 62 g (89% of theory) of (4-nitro-2-trichloromethylphenyl)-n-propyl disulfide as a yellow oil.

Sources & evidence

ORD record
ord-c9e8f74d137b4ad694308298b3cb3d81
Source dataset
uspto-grants-1982_04
Patent number
US04324793

Reaction notes

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