HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitro-2-trichloromethylbenzenesulfenyl chloride → (4-Nitro-2-trichloromethylphenyl)-(2-cyano-3-chlorophenyl)-disulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitro-2-trichloromethylbenzenesulfenyl chloride | HCID 12763555 | — |
| Reactant | 2-Chloro-6-sulfanylbenzonitrile | HCID 21224765 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | (4-Nitro-2-trichloromethylphenyl)-(2-cyano-3-chlorophenyl)-disulfide | HCID 20544198 | 86.3% |
Reaction Steps
30.7 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride in 500 ml of diethyl ether is reacted in a stirred apparatus with 17 g of 2-cyano-3-chlorothiophenol for 4 hours at 30° C. There is obtained 38 g (86% of theory) of (4-nitro-2-trichloromethylphenyl)-(2-cyano-3-chlorophenyl)-disulfide; m.p.: 137° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04324793 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-382f6d68d4254a72a9fb334ed1edad9a |
| Source note | uspto-grants-1982_04 |