HRID2285739

反应详情

EQUATION

反应方程式

HRID 2285739 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

4.8 g of 3-hydroxy-4-carboethoxyphenylguanidine was suspended in 200 ml of chloroform, and 3.9 g of acetylsalicylic acid was added. The mixture was stirred at room temperature for 3 hours. After the reaction, the reaction mixture was cooled, and the resulting crystals were collected by filtration. The crystals were then recrystallized from a mixture of acetone and ligroin.

WORKUP

后处理

  1. customAfter the reaction
  2. temperaturethe reaction mixture was cooled
  3. filtrationthe resulting crystals were collected by filtration
  4. customThe crystals were then recrystallized from a mixture of acetone and ligroin