Sodium Hydroxide → HCID 23679329, compound
Reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][C:10]2([C:13]([OH:15])=[O:14])[CH2:12][O:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Na+:17]>>[C:1]1([CH2:7][CH2:8][CH2:9][C:10]2([C:13]([O-:15])=[O:14])[CH2:12][O:11]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1.[Na+:17]Participants
3
Procedure
5 g of 2-(3-phenylpropyl)oxirane-2-carboxylic acid is dissolved in the equivalent amount of 1 N sodium hydroxide solution, and the resulting aqueous solution is washed once with diethyl ether and evaporated to dryness. The glassy residue, which is dried at 20° C. in vacuo, consists of the pure sodium salt.
Workup
- washthe resulting aqueous solution is washed once with diethyl ether
- customevaporated to dryness
- customThe glassy residue, which is dried at 20° C. in vacuo
Sources & evidence
- ORD record
- ord-d749c28f8e47430e87a3b94672eda7de
- Source dataset
- uspto-grants-1982_04
- Patent number
- US04324796
Reaction notes
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