Sodium 2-(5-phenylpentyl)oxirane-2-carboxylate → HCID 54219, compound

HRID 2285755Notes

Reaction equation

HRID 2285755 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]2([C:15]([O-:17])=[O:16])[CH2:14][O:13]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Na+]>C(OCC)C>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]2([C:15]([OH:17])=[O:16])[CH2:14][O:13]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 1

HCID 23676476Sodium 2-(5-phenylpentyl)oxirane-2-carboxylate

Product 1

HCID 54219HCID 54219, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

3 g of sodium 2-(5-phenylpentyl)oxirane-2-carboxylate are thoroughly shaken with 70 ml of ice-cold 1 N hydrochloric acid and 50 ml of diethyl ether; the organic phase is collected, dried over sodium sulfate and concentrated. 1.7 g of the title compound remain as a viscous, colorless oil.

Workup

  1. customthe organic phase is collected
  2. dry with materialdried over sodium sulfate
  3. concentrationconcentrated

Sources & evidence

ORD record
ord-6586c251bce1453e95f0b94eab96ce9e
Source dataset
uspto-grants-1982_04
Patent number
US04324796

Reaction notes

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