Chloral → HCID 20544536, compound

HRID 2285798Notes

Reaction equation

HRID 2285798 reaction equation
[CH2:1]([NH:4][C:5]([NH2:7])=[O:6])[CH2:2][OH:3].[O:8]=[CH:9][C:10]([Cl:13])([Cl:12])[Cl:11]>>[Cl:11][C:10]([Cl:13])([Cl:12])[CH:9]([NH:7][C:5]([NH:4][CH2:1][CH2:2][O:3][CH:9]([OH:8])[C:10]([Cl:13])([Cl:12])[Cl:11])=[O:6])[OH:8]

Participants

3

Reactant 2

HCID 6407ChloralHCID 73984(2-Hydroxyethyl)urea

Product 1

HCID 20544536HCID 20544536, compound

Procedure

52 g (0.5 mole) of monoethanolurea was heated to 80° C.; 149.0 g (1.01 mole) of chloral was added dropwise thereto between 80°-90° C. with stirring and heated between 80°-90° C. for an additional hour. On cooling, a clear viscous liquid product was obtained that weighed 200 g.

Workup

  1. temperatureheated between 80°-90° C. for an additional hour
  2. temperatureOn cooling
  3. customa clear viscous liquid product was obtained

Sources & evidence

ORD record
ord-e86b4a3da8f342e6b8b05b013a61175b
Source dataset
uspto-grants-1982_04
Patent number
US04324910

Reaction notes

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