Chloral → HCID 20544538, compound

HRID 2285799Notes

Reaction equation

HRID 2285799 reaction equation
[NH2:1][C:2]([NH2:4])=[O:3].[CH:5]([OH:8])([CH3:7])[CH3:6].[O:9]=[CH:10][C:11]([Cl:14])([Cl:13])[Cl:12]>>[Cl:12][C:11]([Cl:14])([Cl:13])[CH:10]([NH:1][C:2]([NH:4][CH2:6][CH:5]([O:8][CH:10]([OH:9])[C:11]([Cl:14])([Cl:13])[Cl:12])[CH3:7])=[O:3])[OH:9]

Participants

3

Reactant 2

HCID 6407ChloralHCID 20544540HCID 20544540, compound

Product 1

HCID 20544538HCID 20544538, compound

Conditions

Temperature
85 °C

Procedure

59 g. (0.5 mole) of monoisopropanol urea was heated to 80° C.; 149.0 g (1.01 moles) of chloral was added dropwise thereto between 80°-90° C. with stirring. After the addition, the reaction mixture was stirred and heated between 80-90° C. for an additional hour. On cooling a clear viscous liquid product was obtained that weighted 205 g.

Workup

  1. additionAfter the addition
  2. stirringthe reaction mixture was stirred
  3. temperatureOn cooling a clear viscous liquid product
  4. customwas obtained that weighted 205 g

Sources & evidence

ORD record
ord-2571232cc8c640c08b8da290fc187f6b
Source dataset
uspto-grants-1982_04
Patent number
US04324910

Reaction notes

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