Ethylene Oxide → HCID 20543074, compound

HRID 2286002Notes

Reaction equation

HRID 2286002 reaction equation
[CH3:1][C:2]1([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])[CH2:11][CH:10]([CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH:9]2[CH:4]([CH2:5][CH2:6][CH2:7][CH2:8]2)[NH:3]1.[CH2:24]1[O:26][CH2:25]1>C(O)CCCCCCC>[OH:26][CH2:25][CH2:24][N:3]1[CH:4]2[CH:9]([CH2:8][CH2:7][CH2:6][CH2:5]2)[CH:10]([CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH2:11][C:2]1([CH3:1])[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]

Participants

4

Procedure

Following the above procedures, 25 grams of 2-methyl-2,4-dihexyl decahydroquinoline in 50 milliliters of 1-octanol was reacted with ethylene oxide at 200° C. for 8 hours to yield 1-(2'-hydroxyethyl)-2-methyl-2,4-dihexyl decahydroquinoline which had a boiling point at 192° C. at 0.7 mm Hg. The products NMR and infrared spectra were consistent with the desired product.

Sources & evidence

ORD record
ord-f5e7a102597f4168ad92ccbeedba2bb3
Source dataset
uspto-grants-1982_04
Patent number
US04326061

Reaction notes

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