HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-formylbenzoate → Ethyl-p-((E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-1-propenyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-formylbenzoate | HCID 80498 | — |
| Reactant | Triphenyl(1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethyl)phosphonium bromide | HCID 11238302 | — |
| Product | Ethyl-p-((E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-1-propenyl)benzoate | HCID 6437076 | — |
Reaction Steps
In a manner analogous to that described in Example 1, from [1-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)ethyl]-triphenylphosphonium bromide and 4-ethoxycarbonylbenzaldehyde there can be obtained p-[(E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)propenyl]-benzoic acid ethyl ester of melting point 90°-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04326055 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-301b0179dbdf421199cfe86744c44a44 |
| Source note | uspto-grants-1982_04 |