HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenyl(1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethyl)phosphonium bromide → HCID 69984079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenyl(1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethyl)phosphonium bromide | HCID 11238302 | — |
| Reactant | Ethyl 4-formyl-2-methylbenzoate | HCID 20543014 | — |
| Product | HCID 69984079 | HCID 69984079 | — |
Reaction Steps
In a manner analogous to that described in Example 1, from [1-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)ethyl]-triphenylphosphonium bromide and 3-methyl-4-ethoxycarbonyl-benzaldehyde there can be obtained p-[(E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)propenyl]-2-methyl-benzoic acid ethyl ester as a colourless oil which is uniform according to thin-layer chromatography, (Rf=0.6; hexane/15% ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04326055 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-719d3081685947a3b29b0df5222e9ffd |
| Source note | uspto-grants-1982_04 |