Morpholine → HCID 86738347, compound
Reaction equation
[CH3:1][C:2]1([CH3:26])[CH2:11][CH2:10][C:9]([CH3:13])([CH3:12])[C:8]2[CH:7]=[C:6](/[C:14](/[CH3:25])=[CH:15]/[C:16]3[CH:24]=[CH:23][C:19]([C:20](O)=[O:21])=[CH:18][CH:17]=3)[CH:5]=[CH:4][C:3]1=2.[NH:27]1[CH2:32][CH2:31][O:30][CH2:29][CH2:28]1>>[CH3:26][C:2]1([CH3:1])[CH2:11][CH2:10][C:9]([CH3:13])([CH3:12])[C:8]2[CH:7]=[C:6](/[C:14](/[CH3:25])=[CH:15]/[C:16]3[CH:24]=[CH:23][C:19]([C:20]([N:27]4[CH2:32][CH2:31][O:30][CH2:29][CH2:28]4)=[O:21])=[CH:18][CH:17]=3)[CH:5]=[CH:4][C:3]1=2Participants
3
Procedure
In a manner analogous to that described in Example 11, from p-[(E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)propenyl]-benzoic acid and morpholine there can be obtained p-[(E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)propenyl]-benzoic acid morpholide of melting point 143°-144° C.
Sources & evidence
- ORD record
- ord-7b9bf506327947758b4b6d8c20a1b22a
- Source dataset
- uspto-grants-1982_04
- Patent number
- US04326055
Reaction notes
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