Adipic Acid → HCID 20542111, compound

HRID 2286150Notes

Reaction equation

HRID 2286150 reaction equation
[Al:1](O)(O)[OH:2].[C:5]([OH:14])(=[O:13])[CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11]>O>[C:5]([O-:14])(=[O:13])[CH2:6][CH2:7][CH2:8][CH2:9][C:10]([O-:12])=[O:11].[OH-:2].[Al+3:1]

Participants

4

Reactant 2

HCID 196Adipic AcidHCID 178526209HCID 178526209, compound

Product 1

HCID 20542111HCID 20542111, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

31.2 g of Al(OH)3 (hydrargillite, 0.4 mol), 116.9 g (0.8 mol) of adipic acid and 300 g of water are initially introduced into a 750 ml sulfonation flask, provided with a reflux condenser, a thermometer and a stirrer, and the mixture is refluxed for 24 hours. After the reaction has ended, the reaction mixture is filtered and the product is washed several times with isopropanol. The product is then dried for 12 hours at 130° C. in a vacuum cabinet. 39.3 g of acicular, crystalline, colourless aluminium monohydroxide adipate result.

Workup

  1. customprovided with a reflux condenser
  2. temperaturea thermometer and a stirrer, and the mixture is refluxed for 24 hours
  3. filtrationthe reaction mixture is filtered
  4. washthe product is washed several times with isopropanol
  5. customThe product is then dried for 12 hours at 130° C. in a vacuum cabinet

Sources & evidence

ORD record
ord-eae3214bdec24b70929395d4f7b0a53a
Source dataset
uspto-grants-1982_04
Patent number
US04327032

Reaction notes

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