反应详情

31.2 g of Al(OH)3 (hydrargillite, 0.4 mol), 116.9 g (0.8 mol) of adipic acid and 300 g of water are initially introduced into a 750 ml sulfonation flask, provided with a reflux condenser, a thermometer and a stirrer, and the mixture is refluxed for 24 hours. After the reaction has ended, the reaction mixture is filtered and the product is washed several times with isopropanol. The product is then dried for 12 hours at 130° C. in a vacuum cabinet. 39.3 g of acicular, crystalline, colourless aluminium monohydroxide adipate result.

1. customprovided with a reflux condenser
2. temperaturea thermometer and a stirrer, and the mixture is refluxed for 24 hours
3. filtrationthe reaction mixture is filtered
4. washthe product is washed several times with isopropanol
5. customThe product is then dried for 12 hours at 130° C. in a vacuum cabinet