Allyl bromide → HCID 12836709, compound

HRID 2286194Notes

Reaction equation

HRID 2286194 reaction equation
O.[O:2]=[C:3]1[N:8]([Na])[C:7](=[O:10])[CH:6]=[N:5][NH:4]1.[CH2:11](Br)[CH:12]=[CH2:13]>C(O)CO>[O:2]=[C:3]1[N:8]([CH2:13][CH:12]=[CH2:11])[C:7](=[O:10])[CH:6]=[N:5][NH:4]1

Participants

4

Reactant 2

HCID 7841Allyl bromideHCID 178526941HCID 178526941, compound

Product 1

HCID 12836709HCID 12836709, compound

Reagents, catalysts & solvents 1

HCID 174Ethylene GlycolSolvent

Conditions

Temperature
80 °C

Procedure

A mixture of 6.12 g 3,5-dioxo-4-sodio-2,3,4,5-tetrahydro-1,2,4-triazine monohydrate, 5.81 g allyl bromide and 50 ml ethylene glycol was heated to 80° C. for 4 hours.

Sources & evidence

ORD record
ord-e9bad52dffde40a9bbaf78de7bdc4480
Source dataset
uspto-grants-1982_04
Patent number
US04327094

Reaction notes

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