Propargyl bromide → HCID 12836710, compound

HRID 2286195Notes

Reaction equation

HRID 2286195 reaction equation
[O:1]=[C:2]1[N:7]([Na])[C:6](=[O:9])[CH:5]=[N:4][NH:3]1.[CH2:10](Br)[C:11]#[CH:12]>C(O)CO>[O:1]=[C:2]1[N:7]([CH2:12][C:11]#[CH:10])[C:6](=[O:9])[CH:5]=[N:4][NH:3]1

Participants

4

Reactant 2

HCID 7842Propargyl bromideHCID 178516812HCID 178516812, compound

Product 1

HCID 12836710HCID 12836710, compound

Reagents, catalysts & solvents 1

HCID 174Ethylene GlycolSolvent

Conditions

Temperature
80 °C

Procedure

A mixture of 4.59 g 3,5-dioxo-4-sodio-2,3,4,5-tetrahydro-1,2,4-triazine, 4.64 g propargyl bromide and 40 ml ethylene glycol was heated to 80° C. for 3 hours.

Sources & evidence

ORD record
ord-b779295b3534438590360deba82aabc3
Source dataset
uspto-grants-1982_04
Patent number
US04327094

Reaction notes

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