Anthralin → HCID 12923093, compound

HRID 2286250Notes

Reaction equation

HRID 2286250 reaction equation
[OH:1][C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][C:12]=3[OH:17])[CH2:7][C:6]=2[CH:5]=[CH:4][CH:3]=1>C1(C)C=CC=CC=1>[CH:2]1([C:11]2[CH:10]=[CH:9][C:8]3[CH2:7][C:6]4[C:15](=[C:2]([OH:1])[CH:3]=[CH:4][CH:5]=4)[C:14](=[O:16])[C:13]=3[C:12]=2[OH:17])[CH2:15][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

3

Reactant 1

HCID 2202Anthralin

Product 1

HCID 12923093HCID 12923093, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Mixture of 2-dodecyl- and 4-dodecyl-1,8-dihydroxy-9-(10H)anthracenone, Rf -value: 0.59 (Merck prepared TLC-plates 60F-254; mobile phase: toluene without chamber saturation). For comparison: Rf -value of 1,8-dihydroxy-9-(10H)anthracenone=0.53 (same conditions).

Sources & evidence

ORD record
ord-9ed3ed8682694d1d859c3573cf656b04
Source dataset
uspto-grants-1982_04
Patent number
US04327114

Reaction notes

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