HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-[4-(Methylsulfonamido)phenyl]acetate → 1-(2-Cyanophenoxy)-3-beta-(4-methanesulphonamidophenylacetamido)ethylamino-2-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-[4-(Methylsulfonamido)phenyl]acetate | HCID 10038092 | — |
| Reactant | HCID 12841761 | HCID 12841761 | — |
| Product | 1-(2-Cyanophenoxy)-3-beta-(4-methanesulphonamidophenylacetamido)ethylamino-2-propanol | HCID 12841764 | — |
Reaction Steps
In a similar manner using 1.2 g. of 3-(β-aminoethylamino)-1-(2-cyanophenoxy)-2-propanol and 1.29 of ethyl 4-methanesulphonamidophenylacetate as starting materials there is obtained 1-(2-cyanophenoxy)-3-β-(4-methanesulphonamidophenylacetamido)ethylamino-2-propanol, isolated as its oxalate, m.p. 180°-182° C. after crystallisation from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04327113 |
| Source dataset | uspto-grants-1982_04 |
| ORD ID | ord-7dcd4ff3a0de42e498c2fe5b866059a9 |
| Source note | uspto-grants-1982_04 |