Potassium Hydroxide → HCID 53885185, compound

HRID 2286261Notes

Reaction equation

HRID 2286261 reaction equation
[CH3:1][O:2][N:3]=[C:4]([C:7]1[CH:12]=[N:11][CH:10]=[CH:9][N:8]=1)[C:5]#[N:6].[OH-:13].[K+]>CO.O>[CH3:1][O:2][N:3]=[C:4]([C:7]1[CH:12]=[N:11][CH:10]=[CH:9][N:8]=1)[C:5]([NH2:6])=[O:13]

Participants

5

Reactant 2

HCID 14797Potassium HydroxideHCID 133196HCID 133196, compound

Product 1

HCID 53885185HCID 53885185, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Conditions

Temperature
40 °C

Procedure

α-Methoxyiminopyrazineacetonitrile Z-isomer (6.0 g) was dissolved in 35 ml of methanol. A solution of potassium hydroxide (4 g) in 10 ml of water was added and the dark reaction mixture was stirred for 1 hour at a temperature of 40° C. The greater part of the methanol was evaporated under reduced pressure.

Workup

  1. customthe dark reaction mixture
  2. customThe greater part of the methanol was evaporated under reduced pressure

Sources & evidence

ORD record
ord-dfbebaeb871d44c0b0049c0f3de67942
Source dataset
uspto-grants-1982_04
Patent number
US04327213

Reaction notes

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