HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → HCID 21464724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | Diisopropyl Phenylphosphonite | HCID 298723 | — |
| Product | HCID 21464724 | HCID 21464724 | — |
Reaction Steps
158 parts of diisopropoxyphenylphosphine are added slowly to 84 parts of pivaloyl chloride at 50°-60° C., with thorough stirring. Stirring is then continued for two hours, after which the mixture is fractionated under reduced pressure. Isopropyl pivaloyl-phenylphosphinate distils at 119°-121° C./0.5 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04265723 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-3e5f307ff00546ac8b65cb832a3458e0 |
| Source note | uspto-grants-1981_05 |