Potassium Hydroxide → HCID 178464375, compound

HRID 2286311Notes

Reaction equation

HRID 2286311 reaction equation
F[S:2]([CH2:5][CH2:6][N:7]([CH2:15][CH3:16])[C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([CH3:14])[CH:9]=1)(=[O:4])=[O:3].[OH-:17].[K+:18]>O>[K:18][CH:5]([S:2]([OH:17])(=[O:4])=[O:3])[CH2:6][N:7]([CH2:15][CH3:16])[C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([CH3:14])[CH:9]=1

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 21161675N-(2-Fluorosulfonylethyl)-N-ethyl-m-toluidine

Product 1

HCID 178464375HCID 178464375, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

N-(2-Fluorosulfonylethyl)-N-ethyl-m-toluidine (24.5 g, 0.1 m) is stirred in water (200 ml) and potassium hydroxide (10 g) for 1-3 hours at room temperature or until thin-layer chromatography shows the reaction to be complete. The product is not isolated but is used as an aqueous solution in the coupling reaction.

Workup

  1. customthe reaction
  2. customThe product is not isolated
  3. customis used as an aqueous solution in the coupling reaction

Sources & evidence

ORD record
ord-326ca369539344bd85a49fe102a335e2
Source dataset
uspto-grants-1981_05
Patent number
US04265812

Reaction notes

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