Potassium Hydroxide → HCID 178464374, compound

HRID 2286313Notes

Reaction equation

HRID 2286313 reaction equation
F[S:2]([CH2:5][CH2:6][N:7]([CH2:14][CH3:15])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)(=[O:4])=[O:3].[OH-:16].[K+:17]>O>[K:17][CH:5]([S:2]([OH:16])(=[O:4])=[O:3])[CH2:6][N:7]([CH2:14][CH3:15])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 211616872-[Ethyl(phenyl)amino]ethane-1-sulfonyl fluoride

Product 1

HCID 178464374HCID 178464374, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

N-(2-Fluorosulfonylethyl)-N-ethylaniline (22.8 g, (0.1 m) is stirred in water (200 ml) and potassium hydroxide (10 g) for 1-3 hrs. or until thin-layer chromatography shows reaction to be complete. The product is not isolated but is used as an aqueous solution in the coupling reaction.

Workup

  1. customreaction
  2. customThe product is not isolated
  3. customis used as an aqueous solution in the coupling reaction

Sources & evidence

ORD record
ord-b9e95b1c5d9a4eeaad999fd9717574e6
Source dataset
uspto-grants-1981_05
Patent number
US04265812

Reaction notes

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