huagongshe.com
HRID2286315

反应详情

EQUATION

反应方程式

HRID 2286315 的结构方程式

REACTANTS

反应物

2
结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：CC(=O)Nc1ccc(C)c(NCCS(=O)(=O)F)c1
HCID21161676

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)Nc1ccc(C)c(NCC([K])S(=O)(=O)O)c1
HCID178474155

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

N-(2-Fluorosulfonylethyl-2-methyl-5-acetamidoaniline (13.7 g, 0.05 m) is stirred with water (100 ml.) and potassium hydroxide (5.0 g) at room temperature for 2 hrs. when thin-layer chromatography shows reaction to be complete. The aqueous solution is used in the coupling reaction without further isolation.

WORKUP

后处理

  1. customreaction
  2. customThe aqueous solution is used in the coupling reaction without further isolation