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HRID2286335

反应详情

EQUATION

反应方程式

HRID 2286335 的结构方程式

REACTANTS

反应物

2
结构：Cc1[nH]cnc1CSCCN
HCID665568

4-(((2-Aminoethyl)thio)methyl)-5-methylimidazole

C7H13N3S

结构：CN=C(SC)S(=O)(=O)[O-]
HCID86737078

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=NCCSCc1nc[nH]c1C)S(=O)(=O)O
HCID178485004

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

2 次

PROCEDURE

实验过程

A solution of 1.43 g (0.0085 mole) of 2-(5-methyl-4-imidazolylmethylthio)ethylamine in dry acetonitrile (150 ml) was added dropwise, with stirring, to a solution of 1.43 g (0.0084 mole) of 1-methylthio-1-methyliminomethanesulphonate in dry acetonitrile (150 ml) at 50°, giving an immediate white precipitation.

WORKUP

后处理

  1. customgiving
  2. customan immediate white precipitation