HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylurea → Tetrakis(3-methylureidomethyl)phosphonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylurea | HCID 11719 | — |
| Reactant | Tetrakis(hydroxymethyl)phosphonium chloride | HCID 31298 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Tetrakis(3-methylureidomethyl)phosphonium chloride | HCID 23463252 | 100.2% |
Reaction Steps
Reaction of THPC (9.53 g, 0.05 mol) with N-methylurea (14.82 g, 0.2 mol) in toluene (75 ml), following Example 1, gave 20.78 g (100%) of tetrakis(3-methylureidomethyl)phosphonium chloride (I, R=R'=H, R"=CH3, X=Cl) as a brittle amber glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04265945 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-301e7807dc084aa5afc9e09597a01bb1 |
| Source note | uspto-grants-1981_05 |