Triethylamine → HCID 23461459, compound

Participants

Reaction Steps

The same compound is also obtained when a solution of 1.15 g. diphenylacetyl chloride in 5 ml. anhydrous diethyl ether is added dropwise at 0° C. to a solution of 0.35 g. 2-cyanoaziridine and 0.6 g. triethylamine in 15 ml. diethyl ether and the reaction mixture then stirred for 1 hour at 0° C. and for 2 hours at ambient temperature. The precipitated hydrochloride is filtered off with suction (0.7 g.) and the ethereal filtrate is concentrated to a volume of about 10 ml. and shaken out twice with 5 ml. amounts of water. After evaporation of the ethereal phase, there is obtained 1.13 g. of the desired compound.

Provenance & Evidence