HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 23461518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | Butanoic acid, 4-(diethylamino)-4-oxo- (9CI) | HCID 15205 | — |
| Reactant | Aziridine-2-carbonitrile | HCID 118115 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23461518 | HCID 23461518 | — |
Reaction Steps
3.46 g. N,N-Diethylsuccinic acid monoamide and 4.3 g. dicyclohexylcarbodiimide are dissolved in 35 ml. tetrahydrofuran and 1.36 g. 2-cyanoaziridine is added to the resultant suspension. After subsequently stirring for 2 hours in an ice bath and leaving to stand overnight at ambient temperature, the dicyclohexylurea is separated off and the filtrate evaporated. There are thus obtained 2.9 g. 1-(N,N-diethylsuccinamoyl)-2-cyanoaziridine in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04267174 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-8aa44feb152647ef8f51c91e3ee6918d |
| Source note | uspto-grants-1981_05 |