HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 23462418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13060090 | HCID 13060090 | — |
| Product | HCID 23462418 | HCID 23462418 | — |
Reaction Steps
10 g of 3-methyl-6-hydroxymethyl-imidazo-(2,1-b)thiazole prepared as described in one of the methods in Example 26, is refluxed for 2 hours in 100 ml of SOCl2. The solution is then cooled, 50 ml of ether are added to yield 11 g of 3-methyl-6-chloromethyl-imidazo-(2,1-b)thiazole hydrochloride; m.p. 280°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04267339 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-727c2f1682bf41bd8bc140f07adeb124 |
| Source note | uspto-grants-1981_05 |