Participants
| Role | Name | HCID | Charge |
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| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Acetoguanamine | HCID 10949 | — |
| Catalyst | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131712249 | HCID 131712249 | — |
Reaction Steps
A mixture of 40 parts by weight of acetoguanamine, 60 parts by weight of cresol (60% by weight of m-cresol and 40% by weight of p-cresol) and 50 parts by weight of paraformaldehyde was allowed to react in methanol in the presence of sodium hydroxide catalyst to obtain a methanol solution of acetoguanamine-cresol co-condensation resin. A coil was wound using an insulating paper and immersed in said methanol solution under a vacuum of 40 mmHg for one hour. The coil was then dried at 60° C. for 3 hours, then at 100° C. for 2 hours, and immersed in the same epoxy resin composition as used above except for the powdered silica. After immersion under a vacuum of 0.1 mmHg for 30 minutes and subsequent application of an air pressure of 4 kg/cm2, the coil was removed from the resin composition bath and heated at 100° C. for 5 hours, then at 130° C. for 10 hours to harden the resin. The coil thus treated was disposed in a synthetic resin casing and covered at 80° C. with a resin composition containing 100 parts by weight of the above-said epoxy resin composition and 150 parts by weight of powdered silica. After having been defoamed under a vacuum of 5 mmHg for 3 hours, the coil potted with the resin was heated to harden the resin at 130° C. under atmospheric pressure for 15 hours to obtain an integrated resin-molded coil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04268810 |
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| Source dataset | uspto-grants-1981_05 |
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| ORD ID | ord-32a324e44c7e4b819c670a322dbb1e3d |
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| Source note | uspto-grants-1981_05 |
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