HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-4-nitroaniline → Benzamide, 4-amino-N-(4-amino-2-methylphenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-4-nitroaniline | HCID 7337 | — |
| Reactant | 2-Methyl-4-nitroaniline | HCID 7441 | — |
| Reactant | 4-Amino-N-(4-amino-2-methoxyphenyl)benzamide | HCID 13839876 | — |
| Product | Benzamide, 4-amino-N-(4-amino-2-methylphenyl)- | HCID 4667032 | — |
Reaction Steps
By operating as described under (a) above, but using, instead of 202 parts of 2-methoxy-4-nitro-aniline, 183 parts of 2-methyl-4-nitro-aniline, high yields of 4,4'-diamino-2'-methyl-benzanilide were obtained (melting point: 111°-115° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04269769 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-3a7e62b98b4b416680b3508483b847c0 |
| Source note | uspto-grants-1981_05 |