HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane → HCID 178524083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | 2-Acetylbiphenylene | HCID 4347178 | — |
| Reactant | Sodium Hypochlorite | HCID 23665760 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 178524083 | HCID 178524083 | — |
Reaction Steps
2-Biphenylene carboxylic acid is prepared from the oxidation of 2-acetylbiphenylene in dioxane with sodium hypochlorite solution by the process described by W. Baker et al., J. Chem. Soc. 1476 (1954). The acid is refluxed in excess thionyl chloride to produce the acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04269953 |
| Source dataset | uspto-grants-1981_05 |
| ORD ID | ord-26b3e94407ac44998fcbf73b60e3dfcb |
| Source note | uspto-grants-1981_05 |