HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86755488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Ethyl vinyl ether | HCID 8023 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Product | HCID 86755488 | HCID 86755488 | — |
Reaction Steps
After dissolving 12 g of poly-hydroxystyrene (poly(HST)) in 60 ml of THF, 3.6 g of ethylvinylether was added to the solution. The p-toluene sulfonic acid (p-TSA) was added to the mixture in sufficient quality to act as a catalyst, and reacted for 12 hours at room temperature. After 12 hours, the reaction product was slowly dropped into water in a ratio of 5 parts water to one part reaction product, and neutralized using potassium carbonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06083659 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-1b1efc7a64554a3ab83cf634cf2f8ece |
| Source note | uspto-grants-2000_07 |