HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2,4-Dinitrobenzene → HCID 18546600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2,4-Dinitrobenzene | HCID 6 | — |
| Reactant | HCID 18546622 | HCID 18546622 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 18546600 | HCID 18546600 | — |
Reaction Steps
A solution of 4-(10-Hydroxy-2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecyloxy)benzophenone (6.42 g), 2,4-dinitrochlorobenzene (2.42 g) potassium carbonate (2.76 g) and NMP (15 mL) is heated to 75-80° C. for 24 hrs. The solution is further processed as described in Example 2 to give 4-[10-(2,4-dinitrophenoxy)-2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecyloxy]benzophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06084057 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-4ff5fda6c16d498698aafad53f9f130d |
| Source note | uspto-grants-2000_07 |