HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonyl chloride → HCID 70098645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| Reactant | HCID 53917738 | HCID 53917738 | — |
| Product | HCID 70098645 | HCID 70098645 | — |
Reaction Steps
Using procedure 9, (R)-7-(dipropylamino)-5,6,7,8-tetrahydro-2-naphthalenemethanamine (9) was treated with 4-chlorobenzenesulfonyl chloride. Purification by chromatography gave a solid which was crystallized from hexane to give the title compound colorless crystals (m.p. 72° C.). [α]D =+47° (25° C., CH3OH, c=0.6095).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06084130 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-fff0cf47a719484d9d32cf71dcf246f1 |
| Source note | uspto-grants-2000_07 |