Butyl bromide → HCID 18705878, compound

Participants

Reaction Steps

Using procedure 38, 2-(dipropylamino)-2,3-dihydro-6-hydroxy-1H-inden-5-yl trifluoromethanesulfonate (69, 0.38 g, 1 mmol) was treated with bromobutane (0.27 g, 2 mmol). Chromatographic purification yielded pure product 71 as a oil which was converted into the HCl salt and crystallized from EtOAc/hexane to give a white solid (mp 148-149° C.).

Provenance & Evidence