Hydrochloric Acid → HCID 18705803, compound

Participants

Reaction Steps

Using procedure 49, 2-(dipropylamino)-2,3-dihydro-1H-indene-5,6-dicarboxylate (92, 0.35 g, 1.0 mmol) was treated with phenethylamine (0.16 mL, 1.3 mmol). Purification using silica gel, eluting with 3:1 CH2Cl2 /acetone, afforded an oil that was converted to an HCl salt and recrystallized from hot MeOH/EtOAc to give 112 as a white solid (m.p. 235-240° C.).

Provenance & Evidence