Hydrochloric Acid → HCID 18705903, compound

Participants

Reaction Steps

Using procedure 49, 2-(dipropylamino)-2,3-dihydro-1H-indene-5,6-dicarboxylate (92, 0.3 g, 1.0 mmol) was treated with benzylamine (0.44 mL, 4.0 mmol). Purification on silica gel, eluting with 3:1 hexane/acetone, afforded a solid that was converted to an HCl salt and recrystallized from EtOAc/2-propanol to give 124 as a white solid (m.p. 247-248° C.).

Provenance & Evidence