Benzaldehyde → HCID 689895, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of tert-butyl carbazate (10.0 g, 75.64 mmol) in 99% ethanol (100 ml) was added benzaldehyde (7.64 ml, 75.64 mmol) and the mixture was stirred for 60 min. The mixture was cooled to 0° C., filtered and the precipitate was washed with cold ethanol and dried to give 13.47 g (81%) of N'-benzylidenehydrazinecarboxylic acid tert-butylester as white crystals.

Provenance & Evidence